| Document Date: 2010-10-27 21:27:55
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City Pangborn / London / Austin / Milwaukee / New York / Fairrust / Oxford / / Company Paras N. A. / Hewlett-Packard / Merck / Perrin D. D. / Amgen / Jonsson N. A. / MeI / Winter S. A. / MacMillan / Ó 2009 Elsevier Ltd. / / Country United States / United Kingdom / / Currency USD / AMD / / / Facility Princeton University / Laboratory Chemicals / California Institute of Technology Mass Spectral / Aldrich Library / / IndustryTerm colorless oil / pharmaceutical agent / chemical yield / metal reduction / gas chromatographs / Organic solutions / aniline systems / offical site / side-products / pale yellow oil / homogeneous solution / chemical shift / organic solution / red-orange oil / sodium metal / metal conditions / neutral aromatic systems / reduction protocol / The resulting solution / corresponding deaminated product / dialkyl aniline product / / Organization q¼quartet / Princeton University / California Institute of Technology Mass Spectral / / Person Bryon Simmons / Edward Arnold / Elmer Paragon / Nick A. Paras / / / Position Tetrahedron Young Investigator / representative / AD guard / Corresponding author / / Product sodium bicarbonate / ammonium chloride / Packard HP-1 / / ProvinceOrState New Jersey / Rhode Island / New York / A. B. / / Technology reduction protocol / two-step protocol / / URL www.elsevier.com/locate/tet / www.DetrolLA.com / /
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A process for the rapid removal of dialkylamino-substituents from aromatic rings. Application to the expedient synthesis of (R)-tolterodine